96 well microplate staining for FDG analysis


 
    1- Resuspend BM, spleen and FL cells in azide-free, Phenol-red- and biotin-free medium supplemented with 10% heat-inactivated FCS. Keep on ice.
    2- Lyse Red Blood Cells with 1 ml RBC lysing medium for 2  min at RT.
    3- Add 5-7 ml of cold medium.
    4- Layer a cushion of .5 ml of FCS at the bottom of the tubes and centrifuge.
    5- Resuspend the cells in medium. (practically, top up to the desired volume with medium)
    6- Aliquot the cells (1-10 X106) in 0.5 ml aliquots in Eppendorf tubes and warm at 37°C for 15 min.
    7- Prepare the 2x hypotonic shock medium: FDG 2mM, Verapamil 100µM, in water. Warm at 37°C.
    8- Mix equal volume of cells in medium with the 2x hypotonic solution.
    9- Place for 2 min at 37°C.
    10- Add 1 ml cold PBS-serum-azide (PBS-S). Chill. Spin down and resuspend in cold PBS-S.
    From now on keep on ice constantly and use only PBS-S.
    11- Place 0.25 to 3 millions cell per well of a 96 U bottom wells plate.
    12- Centrifuge at  1500 rpm for 3 min (below the 4.5 tag on the big bench centrifuge)
    13- Discard the supernatant  in the sink with a quick wrist-forearm  movement.
    14- Gently vortex the whole plate in order to resuspend the cells in the few µl left.
    15- Proceed with the immunostaining.

 

RBC lysing medium:


Ammonium chloride (NH4Cl)  8.29 g   0.155 M
Potassium bicarbonate (KHCO3)  1 g   10mM
EDTA      0.037 g  1mM
H2O      1l.

Filter with 0.45µm filter
aliquot in 100 ml aliquots
filter the solution to be used with 0.2µm filter.